How would I prepare 25mL each of the dilute solutions of 5mL, 10mL and 20mL and is it possible to dilute it too much?

of what? You need to post the entire question.

To prepare dilute solutions of 5mL, 10mL, and 20mL, you would need to dilute a concentrated stock solution. Here's how you can do it:

1. Start with a concentrated stock solution, let's say it has a volume of 100mL and a known concentration.
2. Take 5mL of the stock solution and transfer it to a new container (e.g., a flask or a beaker).
3. Add distilled water to the container until the total volume reaches 25mL. Mix the solution thoroughly. This will be your 5mL dilute solution.
4. Similarly, repeat the process for the 10mL and 20mL dilute solutions. Take 10mL and 20mL of the stock solution, respectively, and add distilled water to each solution until the total volume reaches 25mL. Make sure to mix the solutions well after each dilution.

Now, regarding your question about diluting too much, it is possible to dilute a solution to the point where it becomes difficult to detect the solute. This is called over-dilution or exceeding the solubility limit. For example, if you continue to dilute a solution to the point where the concentration of solute becomes extremely low, it may become challenging to accurately measure or detect the presence of the solute.

However, if you have a pure liquid solute, you can theoretically dilute it infinitely by adding more solvent, as there is no theoretical limit to dilution. But practically, when diluting solutions, you typically aim to achieve a desired concentration range where the solute can still be detected and measured accurately.