Posted by Rachel on Wednesday, October 19, 2011 at 10:07pm.
Would this be the quickest/most efficient method:
Take a small test tube, add roughly 1mL of water. Add a single drop of one of the unknown solutions. If the drop is miscible with water then it is from the aqueous phase; if it sinks to the bottom (or floats) it is the organic layer. Continue with experiment.
That would work, however I would take the a drop from the top layer of the sample, and drop it into water, avoiding contanimating the separated material.
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